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Data analysis Resources
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Experimental Methods
X-ray Photoelectron Spectroscopy. XPS spectra were collected on a PHI Genesis spectrometer using an aluminum anode X-ray source with a photon energy of 1486.6 eV. Survey spectra were collected with a 25 W, 15 kV source producing a 100 µm beam with a scan range of 1100 to 0 eV with a step size of 0.5 eV and pass energy of 280 eV. High resolution spectra were collected with a step size of step size of 0.1 eV and pass energy of 26 eV.
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Acknowledgements
This work was performed in part at the Virginia Tech Surface Analysis Laboratory (RRID:SCR_27504) which is supported by the National Science Foundation under Grant No. CHE-1531834.
If using CasaXPS for data analysis, please cite:
- Fairley, Neal, et al. "Systematic and collaborative approach to problem solving using X-ray photoelectron spectroscopy." Applied Surface Science Advances 5 (2021): 100112.
Data repositories and information
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Experimental Methods
Powder X-ray Diffraction. PXRD spectra were collected on a Rigaku Miniflex 600 spectrometer using an copper anode X-ray source. Diffractograms were collected with a 2 theta range of 3 to 90 at a speed of 15 degrees/min and step size of 1.
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Acknowledgements
This work was performed in part at the Virginia Tech Surface Analysis Laboratory (RRID:SCR_27504)
Sample Preparation Guides
Additional Guides and Manuals *************
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Experimental Methods
X-ray Absorption Fine Structure / X-ray Emission Spectroscopy. XAFS / XES spectra were collected on a (easyXAFS easyXES150 / easyXAFS Brimstone) spectrometer using a tungsten anode X-ray source. Spectra were collected with 70W from on the Fe K edge with 0.25 eV steps for a duration of 2 seconds per point.
Replace the bold and underlined sections with information from the General Measurement settings.